페놀 수지의 경화 공정

이윤배; 성시창; 신은정; Yoon Bae Lee; Si Chang Sung; Eun Jung Shin

Journal of the Korean Industrial and Engineering Chemistry, Vol.16, No.2, 292-295, April, 2005

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페놀 수지의 경화 공정

Curing Process of Phenolic Resin

이윤배^†, 성시창, 신은정

순천향대학교 화학공학과

Yoon Bae Lee^†, Si Chang Sung, and Eun Jung Shin

Department of Chemical Engineering, Soonchunhyang University, 646 Upnari, Shingchangmyun, Asan-si, Chungchungnam-do 336-745, Korea

E-mail:

초록

자동차 브레이크 패드 만들 때 페놀 수지의 경화 시간은 원가 질감의 중요한 요인이 된다. 이 경화 시간은 페놀수지와 경화제인 Hexamethylenetetramine의 반응 시간을 측정함으로써 알 수 있다. 이 반응 시간은 적외선 분광법(FT-IR), 열치사 주사법(DSC) 및 열중량 분석법(TGA)에 의하여 화학 반응의 완결을 추적하여 알아낼 수 있었다.

The curing time of the phenolic resin for the processing of brake pad is very important factor for reducing the processing cost. The curing time could be investigated by examining the reaction time of the phenolic resin and hexamethylenediamine. The reaction time has been studied by FT-IR, Differential Scanning Calolimetric Analysis (DSC), and Thermogravimetric Analysis (TGA)

Keywords:phenolic resin;curing time;FT-IR;DSC,;TGA

[References]

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Mark H, Othmer D, Overberger C, Seaborg G, Encyclopedia of Chemical Technology, 3rd ed., Vol. 17, p. 384, John Wiley & Sons, NY (1982)
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Mathur RB, Thiyagarajan P, Dhami TL, Carbon Science, 5, 6 (2004)
Jafari SH, Fallanhzadeh F, Rana SK, Iran. Polym. J., 8, 143 (1999)
Bender HL, Mod. Plast., 30, 136 (1953)
Zahs Y, Jo J, Racher D, Pearce E, J. Appl. Polym. Sci., 27, 913 (1982)
Hurst R, Grant D, Hoff R, Burke W, J. Polym. Sci. A: Polym. Chem., 1, 2091 (1965)
He G, Riedl B, Wood Sci. Technol., 38, 69 (2004)
Laskoski M, Kellers TM, Polym. Prep., 45, 720 (2004)
Bindu RL, Nair CPR, Ninan KN, J. Polym. Sci. A: Polym. Chem., 38(3), 641 (2000)
Kamal M, Sourour S, Polym. Eng., 13, 59 (1973)
Lee YK, Kim DJ, Kim HJ, Hwang TS, Rafailovich M, Sokolov J, J. Appl. Polym. Sci., 89(10), 2589 (2003)

[1] Mark H, Bikales N, Overberger C, Menges G, Encyclopedia of Polymer Science and Engineering, Vol. 11, p. 45, John Wiley Sons, NY (1988)

[2] Mark H, Othmer D, Overberger C, Seaborg G, Encyclopedia of Chemical Technology, 3rd ed., Vol. 17, p. 384, John Wiley & Sons, NY (1982)

[3] Gerhartz W, Ullmann's Encyclopedia of Industrial Chemistry, 5th ed. Vol. A19, p. 371, VCH, Berlin (1991)

[4] Knop A, Scheib W, Chemistry and Application of Phenolic Resin, Springer-Verlag, N. Y., (1979)

[5] Mathur RB, Thiyagarajan P, Dhami TL, Carbon Science, 5, 6 (2004)

[6] Jafari SH, Fallanhzadeh F, Rana SK, Iran. Polym. J., 8, 143 (1999)

[7] Bender HL, Mod. Plast., 30, 136 (1953)

[8] Zahs Y, Jo J, Racher D, Pearce E, J. Appl. Polym. Sci., 27, 913 (1982)

[9] Hurst R, Grant D, Hoff R, Burke W, J. Polym. Sci. A: Polym. Chem., 1, 2091 (1965)

[10] He G, Riedl B, Wood Sci. Technol., 38, 69 (2004)

[11] Laskoski M, Kellers TM, Polym. Prep., 45, 720 (2004)

[12] Bindu RL, Nair CPR, Ninan KN, J. Polym. Sci. A: Polym. Chem., 38(3), 641 (2000)

[13] Kamal M, Sourour S, Polym. Eng., 13, 59 (1973)

[14] Lee YK, Kim DJ, Kim HJ, Hwang TS, Rafailovich M, Sokolov J, J. Appl. Polym. Sci., 89(10), 2589 (2003)