화학공학소재연구정보센터
홈 로그인 로그아웃 연락처 사이트맵
Journal of Industrial and Engineering Chemistry, Vol.64, 352-366, August, 2018
DOI10.1016/j.jiec.2018.03.036  Export Citation
Eco-friendly process for preparation of biodiesel from WFO over MTSA-Si catalyst: An innovative approach for the utilization of side product
Mehulkumar L. Savaliya1, 2, and Bharatkumar Z. Dholakiya2, †
  • 1Department of Industrial Chemistry, Shree M and N Virani Science College (Autonomous), Yogidham Gurukul, Kalawad Road, Rajkot 360005, Gujarat, India
  • 2Applied Chemistry Department, Sardar Vallabhbhai National Institute of Technology (SVNIT), Ichchhanath, Surat 395007, Gujarat, India
E-mail:
Present work aimed for the synthesis of a promising MTSA-Si catalyst and its application for biodiesel preparation using WFO. It has been illustrated from the experimental results, the most favorable reaction conditions for the biodiesel preparation using WFO are (i) 1:10 oil to methanol molar ratio, (ii) 5% MTSASi catalyst (w/w), (iii) 130 °C reaction temperature and (iv) 10 h reaction time, for the 98.22% yield of biodiesel. The side product raw glycerin was further transformed into the triglycerides over MTSA-Si catalyzed lauric acid esterification. The fuel properties of biodiesel were estimated and correlated fuel standards.
Keywords:Melamine;Crude glycerol;Chlorosulfonation;Waste frying oil;Triglycerides of lauric acid
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