화학공학소재연구정보센터
홈 로그인 로그아웃 연락처 사이트맵
Journal of Industrial and Engineering Chemistry, Vol.20, No.5, 3141-3149, September, 2014
DOI10.1016/j.jiec.2013.11.057  Export Citation
A facile and reliable route to prepare of flower shaped lead sulfide nanostructures from a new sulfur source
Maryam Shakouri-Arani, and Masoud Salavati-Niasari1, †
  • Department of Inorganic Chemistry, Faculty of Chemistry, University of Kashan, Kashan, P.O. Box 87317-51167, Iran
  • 1Institute of Nano Science and Nano Technology, University of Kashan, Kashan, P.O. Box 87317-51167, Iran
E-mail:
Flower shaped PbS nanostructures were prepared by the solvothermal method using propylene glycol and a new sulfuring agent. Novelty of this work is application of a new thio Schiff-base as complexing and sulfuring agent for synthesizing of PbS nanostructures. SEM and TEM was used to examine the surface morphology of the grown samples; also the products were characterized by XRD, SEAD, UV-vis and FT-IR spectra. The results of this paper indicate that the shape and size of lead sulfide nanocrystals can be controlled systematically by setting certain reaction parameters.
Keywords:Semiconductors;Nanostructures;Electron microscopy;Optical properties;PbS
  1. Link S, Wang ZL, El-Sayed MA, J. Phys. Chem. B, 103(18), 3529 (1999)
  2. Hostetler MJ, Zhong CJ, Yen BKH, Anderegg J, Gross SM, Evans ND, Porter M, Murray RW, J. Am. Chem. Soc., 120(36), 9396 (1998)
  3. Wang Y, Liu H, Toshima H, J. Phys. Chem., 100, 1953 (1996)
  4. Reetz MT, Breinbauer R, Wanniger K, Tetrahedron Lett., 37, 4499 (1996)
  5. Zhang LZ, Sun W, Cheng P, Molecules, 8, 211 (2003)
  6. Soofivand F, Salavati-Niasari M, Mater. Lett., 106, 83 (2013)
  7. Soofivand F, Salavati-Niasari M, Mohandes F, Mater. Lett., 98, 55 (2013)
  8. Bol AA, Meijerink A, J. Lum, 87, 315 (2000)
  9. Gong X, Chen WJ, Wu PF, Chan WK, Appl. Phys. Lett., 73, 2875 (1998)
  10. Bhargava RN, Gallagher D, Hong X, Nurrniko A, Phys. Rev. Lett., 72, 416 (1994)
  11. Sun SH, Murray CB, Weller D, Folks L, Moser A, Science, 287(5460), 1989 (2000)
  12. Hyeon T, Chem. Commun., 927 (2003)
  13. Manna L, Scher EC, Li LS, Alivisatos AP, J. Am. Chem. Soc., 124(24), 7136 (2002)
  14. Gautam UK, Seshadri R, Mater. Res. Bull., 39(4-5), 669 (2004)
  15. Wang SF, Gu F, Lu MK, Zhou GJ, Zhang AY, J. Cryst. Growth, 289(2), 621 (2006)
  16. Saraidarov T, Reisfeld R, Sashchiuk A, Lifshitz E, Physica E, 37, 173 (2007)
  17. Zhang W, Yang Q, Xu L, Yu W, Qian YT, Mater. Lett., 59, 3383 (2005)
  18. Zhou GJ, Lu MK, Xiu ZL, Wang SF, Zhang HP, Zhou YY, Wang SM, J. Phys. Chem. B, 110(13), 6543 (2006)
  19. Zhang ZH, Lee SH, Vittal JJ, Chin WS, J. Phys. Chem. B, 110(13), 6649 (2006)
  20. Ni YH, Wang F, Liu HJ, Yin G, Hong HJ, Ma X, Xu Z, J. Cryst. Growth, 262(1-4), 399 (2004)
  21. Zhang H, Zuo M, Tan S, Li GP, Zhang SY, Nanotechnology, 17, 2931 (2006)
  22. Kuang DB, Xu AW, Fang YP, Liu HQ, Frommen C, Fenske D, Adv. Mater., 15, 747 (2003)
  23. Mo MS, Shao MW, Hu HM, Yang L, Yu WC, Qian YT, J. Cryst. Growth, 244(3-4), 364 (2002)
  24. Lu Q, Gao F, Komarneni S, Nanotechnology, 17, 2574 (2006)
  25. Zhang C, Kang ZH, Shen EH, Wang EB, Gao L, Luo F, Tian CG, Wang CL, Lan Y, Li JX, Cao XJ, J. Phys. Chem. B, 110(1), 184 (2006)
  26. Cornacchio ALP, Jones ND, J. Mater. Chem., 16, 1171 (2006)
  27. Jana S, Goswami S, Nandy S, Chattopadhyay KK, J. Alloy. Compd., 481, 806 (2009)
  28. Salavati-Niasaria M, Sobhani A, Davar F, J. Alloy. Compd., 507, 77 (2010)
  29. Salavati-Niasari M, Davar F, Mater. Lett., 63, 441 (2009)
  30. Davar F, Salavati-Niasari M, Fereshteh Z, J. Alloy. Compd., 496, 638 (2010)
  31. Davar F, Fereshteh Z, Salavati-Niasari M, J. Alloy. Compd., 476, 797 (2009)
  32. Salavati-Niasari M, Loghman-Estarki MR, Davar F, J. Alloy. Compd., 145, 346 (2009)
  33. Salavati-Niasari M, Davar F, Loghman-Estarki MR, J. Alloy. Compd., 494, 199 (2010)
  34. Salavati-Niasari M, Mir N, Davar F, J. Alloy. Compd., 476, 908 (2009)
  35. Salavati-Niasari M, Mir N, Davar F, J. Alloy. Compd., 493, 163 (2010)
  36. Bouropoulos N, Psarras GC, Moustakas N, Chrissanthopoulos A, Baskoutas S, Phys. Status Solidi A-Appl. Res., 205, 2033 (2008)
  37. Baskoutas S, Giabouranis P, Yannopoulos SN, Dracopouios V, Toth L, Chrissanthopoulos A, Bouropoulos N, Thin Solid Films, 515(24), 8461 (2007)
  38. Salavati-Niasari M, Ghanbari D, Davar F, J. Alloy. Compd., 488, 442 (2009)
  39. Salavati-Niasari M, Davar F, Loghman-Estarki MR, J. Alloy. Compd., 481, 776 (2009)
  40. Mohandes F, Davar F, Salavati-Niasari M, J. Mag, 322, 872 (2010)
  41. Salavati-Niasari M, Hosseinzade M, Davar F, J. Alloy. Compd., 509, 134 (2011)
  42. Toedheide K, in: F. Franks (Ed.), Water: A Comprehensive Treatise, vol. 1, Plenum Press, New York, 1972p. 463.
  43. Seward T, Physics M, Chem. Earth, 13, 113 (1981)
  44. Qingqing W, Gang X, Gaorong H, J. Solid State Chem., 178, 2680 (2005)
  45. Zhao XL, Wang CX, Hao XP, Yang JX, Wu YZ, Tian YP, Tao XT, Jiang MH, Mater. Lett., 61, 4791 (2007)
  46. Zhao X, Yu J, Cheng B, Mater. Chem. Phys., 1013, 79 (2007)
  47. Abaker M, Umar A, Baskoutas S, Kim SH, Hwang SW, J. Phys. D-Appl. Phys., 44, 155 (2011)
  48. Baskoutas S, Poulopoulos P, Karoutsos V, Angelakeris M, Flevaris NK, Chem. Phys. Lett., 417(4-6), 461 (2006)
  49. Baskoutas S, Terzis AF, Schommers W, J. Comput. Theoretical Nanoscience, 3, 269 (2006)
  50. Nanda KK, Kruis FE, Fissan H, Nano Lett., 1, 605 (2001)
  51. Salavati-Niasari M, Ghanbari D, Loghman-Estarki MR, J. Polyhedron, 35, 149 (2012)
  52. Bi Y, Lu G, Mater. Lett., 62, 2696 (2008)
  53. Duan T, Lou W, Wang X, Xue Q, Colloids Surf. A: Physicochem. Eng. Asp., 310, 86 (2010)
  54. Nejo OA, Nejo AA, Pullabhotla VSRR, Revaprasadu N, J. Alloy. Compd., 537, 19 (2012)
  55. Wanga D, Yua D, Moa M, Liub X, Qiana Y, Solid State Commun., 125, 475 (2003)
  56. Zhao Z, Zhang K, Zhang J, Yang K, Dong F, Yang B, Colloids Surf. A: Physicochem. Eng. Asp., 355, 114 (2010)
  57. Chen M, Xie Y, Yao ZY, Qian YT, Zhou GE, Mater. Res. Bull., 37(2), 247 (2002)
  58. Salavati-Niasaria M, Ghanbarib D, Particuology, 41, 3 (2012)
  59. Wang S, Pan A, Yin H, He Y, Lei Y, Xu Z, Zou B, Mater. Lett., 60, 1242 (2006)