화학공학소재연구정보센터
학회 한국화학공학회
학술대회 2006년 가을 (10/27 ~ 10/28, 고려대학교)
권호 12권 2호, p.1574
발표분야 미립자공학
제목 Synthesis and Characterization of Flower-shaped ZnO Nanostructures by the Solution Process
초록 Synthesis of flower-shaped ZnO nanostructures ZnO nanorods was achieved by the simple solution process using 0.2M zinc acetate dihydrate and 1M sodium hydroxide in 100ml diionized water at very low temperature about ~90°C in 30 minutes refluxing time. Detailed morphological and optical characterizations demonstrate that the synthesized products are single crystalline with the wurtzite hexagonal phase and grown along the [0001] direction. The composition of as synthesized white powder was analyzed by the IR spectroscopy. Where a standard peak of zinc oxide was observed at 523 cm-1. Raman scattering exhibits a sharp and strong E2 mode at 437 cm-1 which further confirms the crystallinity and wurtzite hexagonal phase for the grown nanostructures. Room-temperature photoluminescence (PL) demonstrate a strong and dominated peak at 381 nm with a suppressed and broad green peak at 515 nm, suggests that the flower-shaped ZnO nanostructures have good optical properties with very less structural defects.
저자 Wahab Rizwan, S. G. Ansari, 김영순, 서형기, 김길성, M. A. Dar, 신형식
소속 전북대
키워드 nanostructures; ZnO
E-Mail
원문파일 초록 보기