화학공학소재연구정보센터
학회 한국화학공학회
학술대회 2011년 가을 (10/26 ~ 10/28, 송도컨벤시아)
권호 17권 2호, p.1434
발표분야 분리기술
제목 Effect of parameters on recrystallization of explosives using supercritical anti-solvent process
초록 The performance and stability of an explosive depend largely on its particle size and particle size distribution. Conventional methods for particle size reduction have drawbacks when they are applied to recrystallization of explosives such as high temperature, ununiform particle size distribution, and contamination by organic solvents. Supercritical fluid recrystallization processes are gaining interests as alternatives to the conventional methods because they can be operated in relatively lower temperature, can produce particles with narrow size distribution, and if carbon dioxide is used, particles without solvent residues can be obtained. Recrystallization of the explosive material by supercritical anti-solvent process is studied. The effect of various parameters are investigated by applying several analyzing methods such as XRD, FT-IR, and Differential Scanning Calorimetry.
저자 서범준1, 이병민1, 이병철2, 김현수3, 이윤우1
소속 1서울대, 2한남대, 3국방과학(연)
키워드 HMX; recrystallization; GAS; supercritical
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