화학공학소재연구정보센터
학회 한국화학공학회
학술대회 2016년 봄 (04/27 ~ 04/29, 부산 BEXCO)
권호 22권 1호, p.739
발표분야 유동층
제목 Optical  characteristics of nano-structured ZnO:Ga powders prepared by a fluidized reactor
초록 Zinc oxide has been understood as one of promising materials to be developed as gas sensing materials by detecting several gases in various different processes. Optical characteristics of ZnO:Ga powders prepared in a continuous and one-step fluidized reactor were investigated. To control the ZnO, Ga3+ was doped into the lattice of host material. The prepared ZnO:Ga powders were analyzed by means of SEM, XRD, DRS and PL. The intensity and shift of main peaks in XRD patterns and crystallite size of ZnO:Ga powders increased with increasing flow rate of micro bubbles(UMB), indicating that the fluidization of micro drops during the formation of powders could help the doping of Ga3+ ions into the lattice of ZnO. The XRD, PL and DRS analyses indicated that Ga3+ was successfully doped into ZnO lattice. The surface morphology of ZnO:Ga powders became more wrinkled and furrowed with increasing UMB, due to the increase of micro shear force and strain. The room temperature photoluminescence indicated that the crystal quality of as-prepared ZnO:Ga powders was getting better with increasing UMB.
저자 임대호1, 유동준1, 전종설1, 양시우1, 이찬기2, 강경민3, 강 용1
소속 1충남대, 2고등기술(연), 3(주) 젠텍
키워드 유동층 반응기 및 공정
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