화학공학소재연구정보센터
학회 한국고분자학회
학술대회 2017년 가을 (10/11 ~ 10/13, 제주컨벤션센터)
권호 42권 2호
발표분야 고분자가공/복합재료
제목 Advanced dehydrate rate of nanocellulose suspension facilitated by tert-Butanol addition in oven drying method
초록 Stock solution of cellulose nanocrystal containing a large amount of water (> 90%), leads to increase of manufacturing cost. Along with several ways for dehydration, oven drying method at high temperature is common one because of its availability and ease, however, the post-drying cellulose nanocrystal powder becomes difficult to redisperse in water in spite of harsh disintegrating treatments. In our study, tert-butanol (t-BuOH) was employed as assisted-drying agent, proved ability not to reduce time only, but t-BuOH also prevents surficial structure of these particles from exfoliation. A 12-folds decrease of drying time was achieved when cellulose nanocrystal solution (1 mL) was mixed with t-BuOH (9 mL) and dried in oven. Shrinkage of cellulose interfibril was also reduced since t-BuOH facilitates the surface tension of water while the residue of t-BuOH keeps nanocellulose particles in distance that make them redispersed well in water because of lack of hydrogen bond forming.
저자 TRAN HONG THANG1, 오동엽2, 황성연2, 박제영2
소속 1KRICT, 2한국화학(연)
키워드 oven drying; tert butanol; cellulose nanocrystal
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