화학공학소재연구정보센터
학회 한국화학공학회
학술대회 2005년 봄 (04/22 ~ 04/23, 여수대학교)
권호 11권 1호, p.312
발표분야 분리기술
제목 Solubility, Density, and Metastable Zone Width of the p-dioxanone- Ethyl Acetate, Tetrahydrofuran and Acetone System
초록 The compound p-dioxanone is used as monomer in the production of poly(p-dioxanone), which have been applied to make biodegradable products, especially surgical devices such as surgical suture, anchors, staples, tacks, clips, plates, screws, and bone fixation devices. Purification of p-dioxanone is also an important step in order to achieve high molecular weight poly(p-dioxanone). Methods for purifying p-dioxanone includes dissolving a crude reaction product containing p-dioxanone in an aliphatic ester solvent, forming crystals of p-dioxanone, and filtering the mixture to recover solids containing crystalline p-dioxanone which is relative pure compared to the crude reaction product. In this work, the solubility and density of p-dioxanone in ethyl acetate was measured over various temperatures. The metastable zone width was measured over cooling rate ranges from 0.01 to 1.0 Kmin-1.
저자 김성일1, 남상욱1, 고주영1, 고재천1, 박소진2, 김철웅1
소속 1한국화학(연), 2충남대
키워드 p-dioxanone; solubility; density; metastable zone
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