학회 |
한국화학공학회 |
학술대회 |
2005년 봄 (04/22 ~ 04/23, 여수대학교) |
권호 |
11권 1호, p.312 |
발표분야 |
분리기술 |
제목 |
Solubility, Density, and Metastable Zone Width of the p-dioxanone- Ethyl Acetate, Tetrahydrofuran and Acetone System |
초록 |
The compound p-dioxanone is used as monomer in the production of poly(p-dioxanone), which have been applied to make biodegradable products, especially surgical devices such as surgical suture, anchors, staples, tacks, clips, plates, screws, and bone fixation devices. Purification of p-dioxanone is also an important step in order to achieve high molecular weight poly(p-dioxanone). Methods for purifying p-dioxanone includes dissolving a crude reaction product containing p-dioxanone in an aliphatic ester solvent, forming crystals of p-dioxanone, and filtering the mixture to recover solids containing crystalline p-dioxanone which is relative pure compared to the crude reaction product. In this work, the solubility and density of p-dioxanone in ethyl acetate was measured over various temperatures. The metastable zone width was measured over cooling rate ranges from 0.01 to 1.0 Kmin-1. |
저자 |
김성일1, 남상욱1, 고주영1, 고재천1, 박소진2, 김철웅1
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소속 |
1한국화학(연), 2충남대 |
키워드 |
p-dioxanone; solubility; density; metastable zone
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E-Mail |
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원문파일 |
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