화학공학소재연구정보센터
Industrial & Engineering Chemistry Research, Vol.49, No.2, 541-547, 2010
Pigmentation of Boc-indanthrone in Organic Solvent/Photopolymer through a Thermal Process
This work explores a pigment converted from a latent pigment in organic solvent and photopolymer through a thermal process. Measurements by thermogravimetric analysis (TGA), ultraviolet-visible (UV-vis) spectroscopy, and Fourier transform infrared (FTIR) spectroscopy showed that regeneration of the pigment from boc-indanthrone in the solvent or photopolymer Could be achieved by heating. X-ray diffraction (XRD) was employed to characterize the regenerated pigments. As shown in the results, the recrystallized Structure is similar to the Structure of the parent pigment. Analysis using field-emission scanning electron microscopy (FESEM) indicated that the particles of the re-formed pigment in the solvent were initially cubic, then aggregated into loose bars, and finally became firmly slated and flat for hydrogen-bonding and pi-pi stacking interactions. In addition, the morphology of the reproduced pigment was found to be Cubic, as in the photopolymer.