Chemistry Letters, Vol.38, No.11, 1018-1019, 2009
Hydrothermal-reduction Synthesis of Ni Nanoparticles by Superrapid Heating Using a Micromixer
Single-phase, high-crystalline, and single-crystalline Ni nanoparticles under 20 nm were continuously prepared through hydrothermal reduction by superrapid heating of Ni(HCOO)(2) Solution using a micromixer in a homogeneous mixture field of H2O and H-2 at 673 K and 30 MPa over 0.5 s.