화학공학소재연구정보센터
Journal of Vacuum Science & Technology A, Vol.27, No.6, 1352-1359, 2009
Transmission electron microscopy specimen preparation perpendicular to the long axis of high aspect ratio features
A new variation of transmission electron microscopy (TEM) specimen preparation is introduced. By thinning a tall high aspect ratio structure perpendicular to the long dimension (i.e., from the side) rather than from perpendicular to the short dimension (either the top or the bottom), it is possible to obtain a more uniformly thin TEM specimen over the entire long dimension of the structure. This article will describe the rational for this variation in specimen preparation. The necessary modifications of four different specimen preparation methods (in situ lift-out, traditional H-bar, ex situ lift-out, and tripod polishing) will be discussed and images of specimens obtained by both of these first two methods will be shown. Additional potential advantages and other applications of this specimen preparation method will be covered. (C) 2009 American Vacuum Society. [DOI: 10.1116/1.3248271]