화학공학소재연구정보센터
Journal of the American Ceramic Society, Vol.92, No.3, 702-709, 2009
Delayed Failure of Hi-Nicalon and Hi-Nicalon S Multifilament Tows and Single Filaments at Intermediate Temperatures (500 degrees-800 degrees C)
Previous results have shown that tows of SiC Nicalon fibers are sensitive to the phenomenon of delayed failure, at temperatures below 700 degrees C. The present paper examines the static fatigue of Hi-Nicalon and Hi-Nicalon S when subjected to constant load, at temperatures between 500 degrees and 800 degrees C in air. Multifilament tows and single filaments were tested. Experimental data show that the rupture times of tows depend on the applied stress according to the conventional power law t sigma(n)=A. In contrast, the stress-rupture time data obtained on single filaments exhibit significant scatter. A model based on slow crack growth in single filaments shows that the stress-rupture of fiber tows follows the conventional time power law. The dependence on temperature was introduced. The model allowed sound calculations of tow lifetimes and characteristics of the slow crack growth phenomenon to be extracted from the tow stress-rupture time data.