Industrial & Engineering Chemistry Research, Vol.48, No.3, 1140-1153, 2009
Monitoring Filtration in Trickle Beds Using Electrical Capacitance Tomography
Experiments were carried out to monitor the evolution of the deposition of fine particles in trickle-bed reactors during the flow of nonpolar hydrocarbon oil-like liquid suspensions using electrical capacitance tomography (ECT) imaging. The accuracy of the ECT rendition was validated in the pristine (i.e., deposit-free) bed state by comparing the liquid holdup measurements from ECT with the liquid holdup from residence time distribution (RTD) measurements. The pulse-flow characteristics (pulse velocity and frequency) estimated from the ECT signals were in agreement with existing literature data. For filtration experiments, the effects of the initial liquid suspension distribution, the gas and liquid superficial velocities, and single-phase flow (i.e., zero gas velocity) on the structure of the deposition in the bed were studied. ECT imaging successfully tracked the unsteady-state progression of bed plugging throughout the trickle bed. It was found that increasing the liquid or gas superficial velocity resulted in increased local deposition. The transition, due to deposition, from trickle to pulse flow was also determined from ECT. In the case of stagnant gas, a filter cake formed on top of the bed.