Chemistry Letters, Vol.36, No.7, 884-885, 2007
Magic-angle-spinning NMR at 30 T with a hybrid magnet
Solid-state NMR measurements at 30T have been performed with a hybrid magnet of National Institute for Materials Science. Spectral resolution less than 3 ppm was confirmed by Br-79 magic-angle-spinning (MAS)NMR measurements of a reference material KBr. A small sample and an aluminum metal shield were used to reduce the effects of field inhomogeneity and fluctuation. As an example of application for an industrial material, Al-27 MAS NMR of a refractory mortar was demonstrated.