Journal of the American Ceramic Society, Vol.83, No.11, 2881-2883, 2000
Microstructure and bending strength of 3Y-TZP/12Ce-TZP ceramics fabricated by liquid-phase sintering at low temperature
With the addition of 1 wt% of MgO-Al2O3-SiO2 glass as a sintering aid, 3Y-TZP/12Ce-TZP ceramics (composed from a mixture of 3Y-TZP and 12Ce-TZP powder) have been fabricated via liquid-phase sintering at 1250 degrees -1400 degreesC. In the sintered bodies, the grain growth of Y-TZP is almost unaffected, whereas that of Ce-TZP is inhibited. MgO . Al2O3 spinel and an amorphous phase that contains Al2O3 and SiO2 (from the sintering aid) fully fill the grain junctions. The bending strength of 3Y-TZP/12Ce-TZP, when sintered at 1250 degrees -1300 degreesC, is similar to 800-900 MPa, which is greater than that of 3Y-TZP ceramics without Ce-TZP particles. Ce-TZP grains and MgO . Al2O3 spinel in 3Y-TZP/12Ce-TZP ceramics may impede crack growth, and the bending strength is enhanced.