Chemical Physics Letters, Vol.354, No.3-4, 193-202, 2002
Proton spectroscopy in solid state nuclear magnetic resonance with windowed phase modulated Lee-Goldburg decoupling sequences
We demonstrate here a new windowed multiple pulse sequence for the detection of protons in solid state NMR. Acquisition windows are inserted in the phase modulated Lee-Goldburg scheme (PMLG). This enables one-dimensional acquisition as against two-dimensional in windowless schemes. The pulse scheme, theoretical justifications and experimental spectra of a few samples are presented. In addition two-dimensional proton-proton and carbon-proton correlation experiments are performed with windowed PMLG proton detection. (C) 2002 Published by Elsevier Science B.V.