화학공학소재연구정보센터
HWAHAK KONGHAK, Vol.39, No.1, 54-58, February, 2001
금속함유 활성탄소섬유에 의한 수중 페놀흡착
Adsorption of Phenol from Aqueous Solution by Metal-containing ACFs
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초록
Ag, Cu와 Co를 각각 1 wt% 함유시킨 석유 핏치계 활성탄소섬유를 제조하고, 이들의 수중 페놀에 대한 흡착능력을 평가하였다. Ag, Cu함유 활성탄소섬유는 20Å미만의 미세공이 발달하는데 비하여 Co함유 활성탄소섬유는 미세공과 함께 30-40Å, 200-300Å의 두 중기공 영역이 발달하였다. 요오드 흡착력은 Ag함유 활성탄소섬유가 우수하였으며, 메틸렌블루와 같은 고분자의 흡착은 Co함유 활성탄소섬유가 효과적이었다. 금속함유 활성탄소섬유의 페놀흡착속도는 활성탄에 비하여 18-180배 빠르며, 제거율도 우수하였다. 파괴점에서 페놀의 흡착량은 금속을 함유하지 않은 활성탄소섬유가 86.4mg/g인데 비하여 Cu함유 활성탄소섬유는 152.4mg/g으로 약 1.8배의 흡착능력을 보였다.
1wt% Ag, Cu and Co-containing Activated Carbon Fibers(ACFs) were prepared and the adsorption abilities of each ACFs for phenol from aqueous solution were investigated. The average pore diameter of Ag and Cu-containing were 20Å, while Co-containing ACF have shown two mesopore regions of 30-40Å and 200-300Å with micropores. Iodine adsorption capacity of Ag-containing ACF is much better than that of other ACFs. The Co-containing ACF with mesopores is more efficient than other adsorbents for the adsorption of polymer such as methyleneblue. The adsorption rate of metal -containing ACFs for phenol is 18-180 times faster than that of Activated Carbon(AC). The adsorption amount of phenol on Cu-ACF at breakpoint was 1.8 times larger than that of non metal-containing ACF.
  1. Mokuokto K, "活性炭 水處理技術과 管理," 신광문화사 (1996)
  2. Donnet JB, Wang TK, Peng JCM, Rebouillat S, "Carbon Fibers," 3rd ed., Marcel Dekker, New York (1998)
  3. Shim JW, Ryu SK, HWAHAK KONGHAK, 36(6), 903 (1998)
  4. Hong EH, Jung YH, Lee KH, Korean J. Chem. Eng., 17(2), 237 (2000)
  5. Oya A, Yoshida S, Alcaniz-Monge J, Linares-Solano A, Carbon, 33, 1085 (1995) 
  6. Ryu SK, Kim SY, Gallego N, Edie DD, Carbon, 37, 1619 (1999) 
  7. Eom SY, Cho TH, Cho KH, Ryu SK, HWAHAK KONGHAK, 38(5), 591 (2000)
  8. 한국산업규격, "KS M 1802"
  9. Mun DC, Lee CK, Lee KH, Kim HS, Shin CS, Kim YK, "Development of Water Treatment Chemical," G7(9-2-1), Chung-buk National Univ. (1997)
  10. Kim HS, Master Dissertation, Chungnam National Univ., Taejon, Korea (1993)
  11. Ruthven DM, "Principles of Adsorption and Adsorption Process," John Wiley & Sons, New York (1984)
  12. Kim HK, Master Dissertation, Chunnam National Univ., Kwangju, Korea (1993)