Transport in Porous Media, Vol.136, No.1, 217-243, 2021
Evidence for the Heterogeneity of the Pore Structure of Rocks from Comparing the Results of Various Techniques for Measuring Hydraulic Properties
We applied three oscillatory methods, the previously presented axial pore-pressure and pore-flow methods, and the laboratory application of the radial oscillatory pore-flow method, and performed steady-state flow-through experiments (Darcy tests), for comparison, in experiments on samples of Westerly granite and Wilkeson sandstone. The granite and the sandstone exhibit pore spaces dominated by micro-fractures and by the granular-medium character with a connected porosity of about 1 and 10 %, respectively. Permeability determined by the axial pore-pressure method shows the closest agreement with the results of the Darcy tests. Apparent porosity and drained modulus derived from specific storage capacity deviate from measured connected porosity and reference values, respectively. The observed deviations of the hydraulic properties between methods suggest that they bear information about the structure of the pore space. Only for the sandstone, anisotropy in hydraulic properties appears to contribute to differences between the results of the various methods. We argue that oscillatory testing provides three indicators for heterogeneity, period dependence, the relation between apparent and connected porosity, and the relation between amplitude ratio and apparent penetration depth, calculated from the simple scaling law for homogeneous materials. These indicators consistently classify the samples of Wilkeson sandstone as hydraulically homogeneous and those of Westerly granite as heterogeneous.
Keywords:Permeability;Porosity;Microstructure;Effective transport properties;Oscillatory pore-pressure method;Oscillatory pore-flow method