Thermal Oxidative Purification of Detonation Nanodiamond in a Gas-Solid Fluidized Bed Reactor

Jae Hoon Lee; Yong Suk Youn; Dong Hyun Lee

Korean Chemical Engineering Research, Vol.56, No.5, 738-751, October, 2018

DOI10.9713/kcer.2018.56.5.738 Export Citation

Thermal Oxidative Purification of Detonation Nanodiamond in a Gas-Solid Fluidized Bed Reactor

Jae Hoon Lee, Yong Suk Youn¹, and Dong Hyun Lee^†

Department of Chemical Engineering, Sungkyunkwan University, 2066, Seobu-ro, Jangan-gu, Suwon-si, Gyeonggi-do, 16419, Korea
¹NanoResource Co., Ltd, 1201, Star valley, 99, Digital-ro 9-gil, Geumcheon-gu, Seoul, 08510, Korea

E-mail:

The effect of the reaction temperature and reaction time on the thermal oxidative purification quality of detonation nanodiamond (NDsoot) was investigated in a gas-solid fluidized bed reactor of a 0.10 m-ID × 1.0 m-high stainless steel column with zirconia beads (dSV = 99.2 μm). The carbon conversion increased with increasing the reaction temperature; however, when the reaction temperature was greater than 773 K, the carbon conversion did not increase. The content of sp3-hybridized carbon at the reaction temperature of 703 K barely changed when the reaction time was more than 30 minutes, but at 773 K, the content decreased as preferred. At 703 K, the purification quality increased with the increasing reaction time; however, at 773 K, the purification quality increased up to 30 minutes and then decreased rapidly.

Keywords:Nanodiamond;Purification;Thermal oxidation;Fluidized bed reactor

[References]

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[2] Chang YR, Lee HY, Chen K, Chang CC, Tsai DS, Fu CC, Lim TS, Tzeng YK, Fang CY, Han CC, Chang HC, Fann W, Nat. Nanotechnol., 3(5), 284 (2008)

[3] Faklaris O, Joshi V, Irinopoulou T, Tauc P, Sennour M, et al., ACS Nano, 3, 3955 (2009)

[4] McGuinness LP, Yan Y, Stacey A, Simpson DA, Hall LT, Maclaurin D, Prawer S, Mulvaney P, Wrachtrup J, Caruso F, Scholten RE, Hollenberg LCL, Nat. Nanotechnol., 6(6), 358 (2011)

[5] Chou CC, Lee SH, Wear, 269, 757 (2010)

[6] Dolmatov VY, Uspekhi Khimii, 70, 687 (2001)

[7] Ivanov MG, Pavlyshko SV, Ivanov DM, Petrov I, Shenderova O, J. Vacuum Science Technology B, 28, 869 (2010)

[8] Kato T, Lin WM, Osawa E, J. Japanese Society Tribologists, 54, 122 (2009)

[9] Shimkunas RA, Robinson E, Lam R, Lu S, Xu XY, Zhang XQ, Huang HJ, Osawa E, Ho D, Biomaterials, 30, 5720 (2009)

[10] Alhaddad A, Adam MP, Botsoa J, Dantelle G, Perruchas G, Gacoin T, Mansuy C, Lavielle S, Malvy C, Treussart F, Bertrand JR, Small, 7, 3087 (2011)

[11] Huang H, Pierstorff, E Osawa E, Ho D, Nano Letters, 7, 3305 (2007)

[12] Zhang XQ, Chen M, Lam R, Xu XY, Osawa E, Ho D, ACS Nano, 3, 2609 (2009)

[13] Chen M, Zhang XQ, Man HB, Lam R, Chow EK, Ho DA, J. Physical Chemistry Letters, 1, 3167 (2010)

[14] Kotov NA, Science, 330(6001), 188 (2010)

[15] Perevedentseva E, Cai PJ, Chiu YC, Cheng CL, Langmuir, 27(3), 1085 (2011)

[16] Krueger A, Chemistry-a European J., 14, 1382 (2008)

[17] Thalhammer A, Edgington RJ, Cingolani LA, Schoepfer R, Jackman RB, Biomaterials, 31, 2097 (2010)

[18] Xing Z, Pedersen TO, Wu XJ, Xue Y, Sun Y, Finne-Wistrand A, Kloss FR, Waag T, Krueger A, Steinmuller-Nethl D, Mustafa K, Tissue Engineering Part A, 19, 1783 (2013)

[19] Shu XZ, Liu YC, Palumbo FS, Lu Y, Prestwich GD, Biomaterials, 25, 1339 (2004)

[20] Yeh J, Ling YB, Karp JM, Gantz J, Chandawarkar A, Eng G, Blumling J, Langer R, Khademhosseini MA, Biomaterials, 27, 5391 (2006)

[21] Shenderova OA, Zhirnov VV, Brenner DW, Crit. Rev. Solid State Mat. Sci., 27, 227 (2002)

[22] Pichot V, Comet M, Fousson E, Baras C, Senger A, Le Normand F, Spitzer D, Diamond Related Materials, 17, 13 (2008)

[23] Osswald S, Yushin G, Mochalin V, Kucheyev SO, Gogotsi Y, J. American Chemical Society, 128, 11635 (2006)

[24] Shenderova O, Koscheev A, Zaripov N, Petrov I, Skryabin Y, Detkov P, Turner S, Van Tendeloo G, J. Phys. Chem. C, 115, 9827 (2011)

[25] Apolonskaya IA, Tyurnina AV, Kopylov PG, Obraztsov AN, Moscow University Physics Bulletin, 64, 433 (2009)

[26] Petit T, Arnault JC, Girard HA, Sennour M, Bergonzo P, Physical Review B, 84, 5 (2011)

[27] Xie FY, Xie WG, Gong L, Zhang WH, Chen SH, Zhang QZ, Chen J, Surface Interface Analysis, 42, 1514 (2010)

[28] Cunningham G, Panich AM, Shames AI, Petrov I, Shenderova O, Diamond Related Materials, 17, 650 (2008)

[29] Xu XY, Yu ZM, Particuology, 10, 339 (2012)

[30] Duffy E, Mitev DP, Thickett SC, Townsend AT, Paull B, Nesterenko PN, Appl. Surf. Sci., 357, 397 (2015)

[31] Petrov I, Shenderova O, Grishko V, Grichko V, Tyler T, Cunningham G, McGuire G, Diamond Related Materials, 16, 2098 (2007)

[32] Liu YY, Kim DY, Electrochimica Acta, 139, 82 (2014)

[33] Zou Q, Wang MZ, Li YG, J. Experimental Nanoscience, 5, 319 (2010)

[34] Pu JC, Wang SF, Sung JC, J. Alloy. Compd., 489, 638 (2010)