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Journal of Supercritical Fluids, Vol.124, 80-89, 2017
Optimized process for recovery of glass- and carbon fibers with retained mechanical properties by means of near- and supercritical fluids
Degradation of hybrid fiber composites using near-critical water or supercritical acetone has been investigated in this study. Process parameters such as temperature (T= 260-300 degrees C), pressure (p = 60-300 bar) and composite/solvent (c/s = 0.29-2.1 g/mL) ratio were varied to determine the effect on the resin degradation efficiency and the quality of the recovered glass and carbon fibers. Supercritical acetone at 260 degrees C, 60 bar and a c/s ratio up to 2.1 g/mL could achieve nearly complete degradation of the resin. The glass fibers were recovered with up to 89% retained tensile strength compared to the virgin glass fibers. The use of near-critical water reduced the tensile strength of the glass fibers by up to 65%, whereas the carbon fibers were recovered with retained tensile strength compared to the virgin carbon fibers using water or acetone. (C) 2017 Elsevier B.V. All rights reserved.