화학공학소재연구정보센터
Journal of Physical Chemistry A, Vol.121, No.3, 669-679, 2017
High-Level ab Initio Predictions for the Ionization Energies, Bond Dissociation Energies, and Heats of Formation of Titanium Oxides and Their Cations (TiOn/TiOn+, n=1 and 2)
The ionization energies (IEs) of TiO and TiO2 and the 0 K bond dissociation energies (Do) and the heats of formation at 0 K (Delta H-f0 degrees) and 298 K (Delta H-f298 degrees) for TiO/TiO+ and TiO2/TiO2+ are predicted by the wave-function-based CCSDTQ/CBS approach. The CCSDTQ/CBS calculations involve the approximation to the complete basis set (CBS) limit at the coupled cluster level up to full quadruple excitations along with the zero-point vibrational energy (ZPVE), high-order correlation (HOC), core-valence (CV) electronic, spin-orbit (SO) coupling, and scalar relativistic (SR) effect corrections. The present calculations yield IE(TiO) = 6.815 eV and are in good agreement with the experimental IE value of 6.819 80 +/- 0.000 10 eV determined in a two-color laser-pulsed field ionization-photoelectron (PFI-PE) study. The CCSDT and MRCI+Qmethods give the best predictions to the harmonic frequencies: omega(e) (omega(+)(e)) = 1013 (1069) and 1027 (1059) cm(-1) and the bond lengths r(e) (r(e)(+)) = 1.625 (1.587) and 1.621 (1.588) angstrom, for TiO (TiO+) compared with the experimental values. Two nearly degenerate, stable structures are found for TiO2 cation: TiO2+(C-2 nu) structure has two equivalent TiO bonds, while the TiO2+(C-s) structure features a long and a short TiO bond. The IEs for the TiO2+(C-2v)<-(TiO2 and TiO2+(C-s)<- TiO2 ionization transitions are calculated to be 9.515 and 9.525 eV, respectively, giving the theoretical adiabatic IE value in good agreement with the experiment IE(TiO2) = 9.573 55 +/- 0.000 15 eV obtained in the previous vacuum ultraviolet (VUV)-PFI-PE study of TiO2. The potential energy surface of TiO2+ along the normal vibrational coordinates of asymmetric stretching mode (omega(+)(3)) is nearly flat and exhibits a double-well potential with the well of TiO2+ (CO situated around the central well of TiO2+(C-2 nu). This makes the theoretical calculation of omega(+)(3) infeasible. For the symmetric stretching (omega(+)(1)), the current theoretical predictions overestimate the experimental value of 829.1 2.0 cm(-1) by more than 100 cm(-1). This work together with the previous experimental and theoretical investigations supports the conclusion that the CCSDTQ/CBS approach is capable of providing reliable IE and D-0 predictions for TiO/TiO+ and TiO2/TiO2+ with error limits less than or equal to 60 meV. The CCSDTQ/CBS calculations give the predictions of D-0(Ti+-O)- D-0(Ti-O) = 0.004 eV and D-0(O-TiO)- D-0(O-TiO+) = 2.699 eV, which are also consistent with the respective experimental determination of 0.008 32 +/- 0.000 10 and 2.753 75 +/- 0.000 18 eV.