This study was designed to investigate the use of commercial adsorbent materials for the removal of nitrogen compounds from a vacuum gas oil obtained from an industrial atmospheric distillation unit. Two types of adsorbents were tested: a clay developed specifically for the removal of nitrogen compounds from middle distillates (jet fuel and diesel); and a silica used in a variety of industries. Kinetic and thermodynamic equilibrium experiments were conducted at three temperatures: 80, 100, and 120 degrees C. The variation in the concentration of nitrogen and aromatic compounds was monitored throughout the kinetic adsorption and thermodynamic equilibrium experiments. When an adsorbent/gas oil mass ratio of 0.75 was used, the clay removed around 70% of the basic nitrogen compounds from the gas oil, while the silica removed 80% of the same compounds, which are the ones that effectively hamper catalytic cracking. The silica also removed 14.2% of the aromatic compounds, while the clay only removed 4.1%. This study shows that it is possible to treat a viscous hydrocarbon feed using an adsorption process to remove nitrogen compounds without the need to dilute the feed. Using a fluidized bed advanced cracking evaluation (ACE) unit, which simulates a fluid catalytic cracking unit on a bench scale, the gas oil treated with silica produced 3% more liquid petroleum gas (LPG) and 4% more gasoline, while the gas oil treated with clay produced 2% more LPG and 3% more gasoline than the untreated gas oil.