A novel polylysine-resorcinol base γ-alumina nanotube hybrid material for effective adsorption/preconcentration of cadmium from various matrices

Nan Xu; Weimin Li; Ming Zhang; Xiaobo Wang

Journal of Industrial and Engineering Chemistry, Vol.46, 157-165, February, 2017

DOI10.1016/j.jiec.2016.10.027 Export Citation

A novel polylysine-resorcinol base γ-alumina nanotube hybrid material for effective adsorption/preconcentration of cadmium from various matrices

Nan Xu^{1, 2}, Weimin Li^{1, 3}, Ming Zhang^{1, 3}, and Xiaobo Wang^{1, 2, †}

¹State Key Laboratory of Solid Lubrication, Lanzhou Institute of Chemical Physics, Chinese Academy of Sciences, Lanzhou 730000, China
²Qingdao Center of Resource Chemistry and New Materials, Lanzhou Institute of Chemical Physics, Chinese Academy of Sciences, Qingdao 266000, China
³, China

E-mail:

Polylysine-resorcinol coated alumina nanotube has been synthesized based on Mannich reaction. Synthetic polymer has been obtained using lysine and resorcinol as monomer and p-formaldehyde as linker by condensation reaction. The nanosorbent was employed for cadmium adsorption from aqueous samples. Effective parameters on sorption process have been optimized with Box-Behnken design (BBD). Equilibrium time was 11 min as well as adsorption capacity was 220 mg g-1. Regeneration of the sorbent was performed with HNO3 solution (0.5 mol L-1). The accuracy of the method was evaluated by determination of cadmium in various real samples.

Keywords:Alumina;Cadmium;Food sample;Polymer nanocomposite

[References]

Lugt PM, Tribol. Trans., 52, 470 (2009)
Huang L, Guo D, Wen SZ, Tribol. Int., 93, 620 (2016)
Cann PME, Damiens B, Lubrecht AA, Tribol. Int., 37, 859 (2004)
Querlioza E, Villea F, Lenonb H, Lubrecht T, Tribol. Int., 40, 1619 (2007)
Lugt PM, Grease Lubrication in Rolling Bearings, first ed., John Wiley & Sons, West Sussex, 2012.
Cen H, Lugt PM, Morales-Espejel G, Tribol. Trans., 57, 668 (2014)
Cen H, Lugt PM, Morales-Espejel G, Tribol. Trans., 57, 1066 (2014)
Morales-Espejel G, Lugt PM, Pasaribu HR, Cen H, Tribol. Int., 74, 7 (2014)
Cyriac F, Lugt PM, Bosman R, Padberg J, Venner H, Tribol. Lett., 61, 18 (2016)
Romanl C, Valencial C, Franco JM, Tribol. Lett., 63, 20 (2016)
Xu N, Li WM, Zhang M, Zhao GQ, Wang XB, RSC Adv., 5, 54202 (2015)
Martın-Alfonso JE, Moreno G, Valencia C, Sanchez MC, Franco JM, Gallegos C, J. Ind. Eng. Chem., 15(5), 687 (2009)
Moreno G, Valencia C, de Paz MV, Franco JM, Gallegos C, Ind. Eng. Chem. Res., 45(11), 4001 (2006)
Salomonsson L, Stang G, Zhmud B, Tribol. Trans., 50, 302 (2007)
Delgado MA, Valencia C, Sanchez MC, Franco JM, Gallegos C, Tribol. Lett., 23, 47 (2006)
Delgado MA, Sanchez MC, Valencia C, Franco JM, Gallegos C, Chem. Eng. Res. Des., 83(A9), 1085 (2005)
Kaskhedikar N, Karatas Y, Cui G, Maier J, Wiemhofer HD, J. Mater. Chem., 21, 11838 (2011)
Kato Y, Ishihara T, Ikuta H, Uchimoto Y, Wakihara M, Angew. Chem.-Int. Edit., 43, 1966 (2004)
Kato Y, Suwa K, Ikuta H, Uchimoto Y, Wakihara M, Yokoyama S, Yabe T, Yamamoto M, J. Mater. Chem., 13, 280 (2003)
Jaiswal V, Kalyani RB, Rastogi R, Kumar J, J. Mater. Chem. A, 2, 10424 (2014)
HO TL, Chem. Rev., 75, 1 (1975)
Yan JC, Zeng XQ, van der Heide E, Ren TH, Zhao YD, RSC Adv., 4, 20940 (2014)
Strohmeier BR, Appl. Surf. Sci., 40, 249 (1989)
Tan BJ, Klabunde KJ, Sherwood PMA, Chem. Mater., 2, 186 (1990)
Allen GC, Hallam KR, Appl. Surf. Sci., 93, 25 (1996)
Larkin P, Infrared and Raman Spectroscopy: Principles and Spectral Interpretation, Elsevier, Oxford, 2011.
Gouin X, Grange P, Bois L, L’Haridon P, Laurent Y, J. Alloy. Compd., 224, 22 (1995)

[1] Lugt PM, Tribol. Trans., 52, 470 (2009)

[2] Huang L, Guo D, Wen SZ, Tribol. Int., 93, 620 (2016)

[3] Cann PME, Damiens B, Lubrecht AA, Tribol. Int., 37, 859 (2004)

[4] Querlioza E, Villea F, Lenonb H, Lubrecht T, Tribol. Int., 40, 1619 (2007)

[5] Lugt PM, Grease Lubrication in Rolling Bearings, first ed., John Wiley & Sons, West Sussex, 2012.

[6] Cen H, Lugt PM, Morales-Espejel G, Tribol. Trans., 57, 668 (2014)

[7] Cen H, Lugt PM, Morales-Espejel G, Tribol. Trans., 57, 1066 (2014)

[8] Morales-Espejel G, Lugt PM, Pasaribu HR, Cen H, Tribol. Int., 74, 7 (2014)

[9] Cyriac F, Lugt PM, Bosman R, Padberg J, Venner H, Tribol. Lett., 61, 18 (2016)

[10] Romanl C, Valencial C, Franco JM, Tribol. Lett., 63, 20 (2016)

[11] Xu N, Li WM, Zhang M, Zhao GQ, Wang XB, RSC Adv., 5, 54202 (2015)

[12] Martın-Alfonso JE, Moreno G, Valencia C, Sanchez MC, Franco JM, Gallegos C, J. Ind. Eng. Chem., 15(5), 687 (2009)

[13] Moreno G, Valencia C, de Paz MV, Franco JM, Gallegos C, Ind. Eng. Chem. Res., 45(11), 4001 (2006)

[14] Salomonsson L, Stang G, Zhmud B, Tribol. Trans., 50, 302 (2007)

[15] Delgado MA, Valencia C, Sanchez MC, Franco JM, Gallegos C, Tribol. Lett., 23, 47 (2006)

[16] Delgado MA, Sanchez MC, Valencia C, Franco JM, Gallegos C, Chem. Eng. Res. Des., 83(A9), 1085 (2005)

[17] Kaskhedikar N, Karatas Y, Cui G, Maier J, Wiemhofer HD, J. Mater. Chem., 21, 11838 (2011)

[18] Kato Y, Ishihara T, Ikuta H, Uchimoto Y, Wakihara M, Angew. Chem.-Int. Edit., 43, 1966 (2004)

[19] Kato Y, Suwa K, Ikuta H, Uchimoto Y, Wakihara M, Yokoyama S, Yabe T, Yamamoto M, J. Mater. Chem., 13, 280 (2003)

[20] Jaiswal V, Kalyani RB, Rastogi R, Kumar J, J. Mater. Chem. A, 2, 10424 (2014)

[21] HO TL, Chem. Rev., 75, 1 (1975)

[22] Yan JC, Zeng XQ, van der Heide E, Ren TH, Zhao YD, RSC Adv., 4, 20940 (2014)

[23] Strohmeier BR, Appl. Surf. Sci., 40, 249 (1989)

[24] Tan BJ, Klabunde KJ, Sherwood PMA, Chem. Mater., 2, 186 (1990)

[25] Allen GC, Hallam KR, Appl. Surf. Sci., 93, 25 (1996)

[26] Larkin P, Infrared and Raman Spectroscopy: Principles and Spectral Interpretation, Elsevier, Oxford, 2011.

[27] Gouin X, Grange P, Bois L, L’Haridon P, Laurent Y, J. Alloy. Compd., 224, 22 (1995)