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Journal of Supercritical Fluids, Vol.112, 143-152, 2016
The effect of pressurized and fast stabilization on one step batch foaming process for the investigation of cell structure formation
Control of cell structure during pressure drop is essential for the investigation of cell formation mechanism. In this work, a one step batch foaming setup was totally redesigned to stabilize foam structure at initial stages of cell forming during and after depressurization as a novel idea. The saturation pressure, duration of pressure drop and foaming temperatures were 18.5 MPa, 100 ms and 70, 90, 110 degrees C, respectively. The shortest stabilized foaming time was 5 ms and the longest was 5000 ms. For comparison purposes non-stabilized samples were also produced. It was concluded that the effect of stabilization on foam morphology is dependent on the foaming temperature. Foam structure at foaming temperatures of 70 degrees C did not change with change of foaming time significantly. Foam structure at foaming temperatures of 110 degrees C for the shortest and the longest foaming times changed from 90 mu m to 170 mu m and 7E + 06 cell/cm(3) to 8E + 06 cell/cm(3). (C) 2015 Elsevier B.V. All rights reserved.