In this study, we experimentally investigate sedimentation of concentrated (30% in volume) bidisperse suspensions using a laser-induced fluorescence technique. Particles were of same density and mixed in 1:1 ratio. The small-to-large-particle ratio varied from 032 to 0.63. We firstly show that the experimental downward velocities of interfaces are well predicted by the MLB theory and that the Smith effect is less important when the size ratio is increased. We secondly show the sedimentation process to follow a particular type depending on such size ratio. In particular, type 3 is involved at the highest size ratio and for which the mixed zone is connected to the sediment through a rarefaction fan. However, by lowering the size ratio to 032, the sedimentation type is found to be then type 1 where no rarefaction fan does exist. These experimental findings are in qualitative agreement with the predictions of Dorrell and Hogg. Finally sediment structure was examined and its constitution was evaluated in the course of time, showing the occurrence of the transition from mixed sediment to mono-sized sediment. The dependence of such a transition and the mixing level on the size ratio was found to agree with theoretical predictions from literature. (C) 2015 Elsevier B.V. All rights reserved.