Materials Chemistry and Physics, Vol.165, 134-141, 2015
Synthesis and characterization of large WO3 sheets synthesized by resistive heating method
A simple, low-cost method is presented to grow tungsten oxide large sheets simply by resistively heating a pure tungsten filament under air/water vapor flow. The obtained structures were studied using scanning and transmission electron microscopy, selected area diffraction, X Ray diffraction, Raman and X-ray photoelectron spectroscopy, photoluminescence and zeta potential measurements. SEM observations revealed that sheets formed by broadening of the wires/belts over longer growth period. Photoluminescence measurements showed that tungsten oxide sheets had an intense visible emission band. (C) 2015 Published by Elsevier B.V.