Vacuum spray drying is a new technique used to produce concentrated orange juice powder using maltodextrin as a drying agent. The dryer was developed for the low-temperature (40-50 degrees C) drying powderization of liquefied food using superheated steam (200 degrees C) as a heating medium. The physicochemical properties of orange juice powder with four different combinations of juice solids: maltodextrin solids at 60:40, 50:50, 40:60, and 30:70 were determined. The moisture content, hygroscopicity, water activity, particle size, particle morphology, color characteristics, rehydration and ascorbic acid retention were significantly affected by the maltodextrin concentration and drying conditions. Water sorption and the glass transition temperature of orange juice powder conditioned at various water activities were also evaluated. The obtained data were well fitted to both BET and GAB models. A strong plasticizing effect of water on Tg was able to predicted by the Gordon Taylor model, where Tg was greatly reduced by the increasing moisture content of the powder. (C) 2015 Elsevier Ltd. All rights reserved.