Preparation of isotropic pitch-based carbon fiber using hyper coal through co-carbonation with ethylene bottom oil

Jianxiao Yang; Koji Nakabayashi; Jin Miyawaki; Seong-Ho Yoon

Journal of Industrial and Engineering Chemistry, Vol.34, 397-404, February, 2016

DOI10.1016/j.jiec.2015.11.026 Export Citation

Preparation of isotropic pitch-based carbon fiber using hyper coal through co-carbonation with ethylene bottom oil

Jianxiao Yang¹, Koji Nakabayashi², Jin Miyawaki^{1, 2}, and Seong-Ho Yoon^{1, 2, †}

¹Interdisciplinary Graduate School of Engineering Science, Kyushu University, 6-1 Kasugakoen, Kasuga, Fukuoka, Japan
²Institute for Materials Chemistry and Engineering, Kyushu University, 6-1 Kasugakoen, Kasuga, Fukuoka, Japan

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A spinnable pitch was developed from the tetrahydrofuran-soluble fractions (THFS) of hyper coal (HPC) and used to prepare carbon fibers. THFS-derived pitch from bituminous coal-derived HPC showed excellent spinnability and the obtained carbon fibers had a tensile strength of over 800 MPa with a diameter of 13 mm following heat treatment at 800 8C for 5 min. Thus, HPC was shown to be a useful alternative precursor for the preparation of low-cost and general-performance carbon fibers.

Keywords:Hyper coal (HPC);Ethylene bottom oil;co-carbonization;Spinnable isotropic pitch;Pitch-based carbon fiber

[References]

Frank E, Steudle LM, Ingildeev D, Sporl JM, Buchmeiser MR, Angew. Chem.-Int. Edit., 53, 5262 (2014)
Baker DA, Rials TG, J. Appl. Polym. Sci., 130(2), 713 (2013)
Sudo K, Shimizu K, J. Appl. Polym. Sci., 44, 127 (1992)
Kadla JF, Sudo S, Venditti RA, Gilbert RD, Compere AL, Griffith W, Carbon, 40, 2913 (2002)
Baker DA, Gallego NC, Baker FS, J. Appl. Polym. Sci., 124(1), 227 (2012)
Ma XJ, Zhao G, J. Wood Sci. Technol., 44, 3 (2010)
Li DN, Ma XJ, Cellulose, 20, 1649 (2013)
Prauchner MJ, Pass VMD, Otani S, Otani C, Carbon, 43, 591 (2005)
Qiao WM, Huda M, Song Y, Yoon SH, Korai Y, Mochida I, Katou O, Hayashi H, Kawamoto K, Energy Fuels, 19(6), 2576 (2005)
Berrueco C, Alvarez P, Diez N, Granda M, Menendez R, Blanco C, Santamaria R, Millan M, Fuel, 101, 9 (2012)
Okuyama N, Komatsu N, Shigehisa T, Kaneko T, Tsutuya S, Fuel Process. Technol., 85(8-10), 947 (2004)
Takanohashi T, Shishido T, Kawashima H, Saito I, Fuel, 87(4-5), 592 (2008)
Hamaguchi M, Okuyam N, Tanso, 257, 149 (2013)
Mishra A, Saha M, Bhatia G, Aggarwal RK, Raman V, Yadav HS, J. Mater. Process. Technol., 168, 316 (2005)
Drbohlav J, Stevenson WTK, Carbon, 33, 693 (1995)
Yoon SH, Korai Y, Mochida I, Carbon, 32, 281 (1994)
Derbyshire F, Andrews R, Jacques D, Jagtoyen M, Kimber G, Rantell T, Fuel, 80(3), 345 (2001)
Prauchner MJ, Pass VMD, De Menezes SMC, J. Wood Chem. Technol., 21, 371 (2001)

[Referenced By]

[1] Frank E, Steudle LM, Ingildeev D, Sporl JM, Buchmeiser MR, Angew. Chem.-Int. Edit., 53, 5262 (2014)

[2] Baker DA, Rials TG, J. Appl. Polym. Sci., 130(2), 713 (2013)

[3] Sudo K, Shimizu K, J. Appl. Polym. Sci., 44, 127 (1992)

[4] Kadla JF, Sudo S, Venditti RA, Gilbert RD, Compere AL, Griffith W, Carbon, 40, 2913 (2002)

[5] Baker DA, Gallego NC, Baker FS, J. Appl. Polym. Sci., 124(1), 227 (2012)

[6] Ma XJ, Zhao G, J. Wood Sci. Technol., 44, 3 (2010)

[7] Li DN, Ma XJ, Cellulose, 20, 1649 (2013)

[8] Prauchner MJ, Pass VMD, Otani S, Otani C, Carbon, 43, 591 (2005)

[9] Qiao WM, Huda M, Song Y, Yoon SH, Korai Y, Mochida I, Katou O, Hayashi H, Kawamoto K, Energy Fuels, 19(6), 2576 (2005)

[10] Berrueco C, Alvarez P, Diez N, Granda M, Menendez R, Blanco C, Santamaria R, Millan M, Fuel, 101, 9 (2012)

[11] Okuyama N, Komatsu N, Shigehisa T, Kaneko T, Tsutuya S, Fuel Process. Technol., 85(8-10), 947 (2004)

[12] Takanohashi T, Shishido T, Kawashima H, Saito I, Fuel, 87(4-5), 592 (2008)

[13] Hamaguchi M, Okuyam N, Tanso, 257, 149 (2013)

[14] Mishra A, Saha M, Bhatia G, Aggarwal RK, Raman V, Yadav HS, J. Mater. Process. Technol., 168, 316 (2005)

[15] Drbohlav J, Stevenson WTK, Carbon, 33, 693 (1995)

[16] Yoon SH, Korai Y, Mochida I, Carbon, 32, 281 (1994)

[17] Derbyshire F, Andrews R, Jacques D, Jagtoyen M, Kimber G, Rantell T, Fuel, 80(3), 345 (2001)

[18] Prauchner MJ, Pass VMD, De Menezes SMC, J. Wood Chem. Technol., 21, 371 (2001)