화학공학소재연구정보센터
Korean Journal of Materials Research, Vol.24, No.11, 585-590, November, 2014
EBSD측정에 의한 반복겹침접합압연된 무산소동의 두께방향으로의 미세조직 변화 분석
Microstructural Evolution Analysis in Thickness Direction of An Oxygen Free Copper Processed by Accumulative Roll-Bonding Using EBSD Measurement
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Microstructural evolution in the thickness direction of an oxygen free copper processed by accumulative rollbonding (ARB) is investigated by electron back scatter diffraction (EBSD) measurement. For the ARB, two copper alloy sheets 1 mm thick, 30 mm wide and 300 mm long are first degreased and wire-brushed for sound bonding. The sheets are then stacked and roll-bonded by about 50% reduction rolling without lubrication at an ambient temperature. The bonded sheet is then cut to the two pieces of the same dimensions and the same procedure was repeated on the sheets up to eight cycles. The specimen after 1 cycle showed inhomogeneous microstructure in the thickness direction so that the grains near the surface were finer than those near the center. This inhomogeneity decreased with an increasing number of ARB cycles, and the grain sizes of the specimens after 3 cycles were almost identical. In addition, the aspect ratio of the grains decreased with an increasing number of ARB cycles due to the subdivision of the grains by shear deformation. The fraction of grains with high angle grain boundaries also increased with continuing process of the ARB so that it was higher than that of the low angle grain boundaries in specimens after 3 cycles. A discontinuous dynamic recrystallization occurred partially in specimens after 5 cycles.
  1. Valiev RZ, Krasilnikov NA, Tsenev NK, Mater. Sci. Eng. A-Struct. Mater. Prop. Microstruct. Process., 137, 35 (1991)
  2. Abdulov RZ, Valiev RZ, Krasilnilov NA, Mater. Sci. Lett., 9, 1445 (1990)
  3. Saito Y, Tsuji N, Utsunomiya H, Sakai T, Hong RG, Scr. Mater., 39, 1221 (1998)
  4. Tsuji N, Saito Y, Utsunomiya H, Tanigawa S, Scr. Mater., 40, 795 (1999)
  5. Lee SH, Saito Y, Tsuji N, Utsunomiya H, Sakai T, Scr. Mater., 46, 281 (2002)
  6. Lee SH, Saito Y, Sakai T, Utsunomiya H, Mater. Sci. Eng. A-Struct. Mater. Prop. Microstruct. Process., 325, 228 (2002)
  7. Lee SH, Saito Y, Park KT, Shin DH, Mater. Trans., 43, 2320 (2002)
  8. Lee SH, Inagaki H, Utsunomiya H, Saito Y, Sakai T, Mater. Trans., 44, 1376 (2003)
  9. Saito Y, Utsunomiya H, Suzuki H, Proc. Inst. Mech. Eng. Ser. B, 215, 947 (2001)
  10. Sakai T, Saito Y, Kanzaki T, Tamaki N, Tsuji N, J. JCBRA, 40, 213 (2001)
  11. Huang X, Tsuji N, Hansen N, Minamino Y, Mater. Sci. Eng. A-Struct. Mater. Prop. Microstruct. Process., 340, 265 (2003)
  12. Lee SH, Cho J, Han SZ, Lim CY, Korean J. Mater. Res., 15(4), 240 (2005)
  13. Lee SH, Cho J, Lee CH, Han SZ, Lim CY, Korean J. Mater. Res., 15(9), 555 (2005)
  14. Lim CY, Han SZ, Lee SH, Met. Mater. Ineter., 12, 225 (2006)
  15. Lee SH, Han SZ, Lim CY, Korean J. Mater. Res., 16(9), 592 (2006)
  16. Lee SH, Kim CS, Kim SS, Han SZ, Lim CY, Korean J. Mater. Res., 17(7), 361 (2007)
  17. Lee SH, Han SZ, Kim HW, Lim CY, Korean J. Mater. Res., 19(8), 432 (2009)
  18. Lee SH, Kim HW, Lim CY, J. Nanosci. Nanotechnol., 11, 1613 (2011)
  19. Lee SH, Kim HW, Lim CY, J. Nanosci. Nanotechnol., 11, 1459 (2011)