It is important to determine the residence time distribution (RTD) of a mill in order to predict the performance of the mill. In this study, the residence time distribution of a continuous centrifugal mill was measured experimentally by using aluminum powder as a tracer in a dry-grinding environment. Aluminum powder was placed into the continuous centrifugal mill chamber as a pulse under a steady-state condition, and then, the discharge time and proportional concentration of the tracer was measured using a metal detector at various G/D ratios and feed rates. During the measurement procedure, the mill product was collected and analyzed with regard to the size distribution to investigate the relationship between the mill product and the characteristics of RTD. In addition, the mill hold-up data was also analyzed after measurement. These test results can be used to predict the mill product size distribution in combination with a kinetic grinding model. (C) 2010 Elsevier Ltd. All rights reserved.