Korean Journal of Materials Research, Vol.12, No.9, 696-700, September, 2002
고온자전합성과 확산 열처리를 이용한 V 이 첨가된 TiAl계 금속간화합물 복합판재의 제조
Formation of a V-Added Ti Aluminide Multilayered Sheet by Self-Propagating High-Temperature Synthesis and Diffusion Annealing
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The Ti-aluminide intermetallic compound was formed from high purity elemental Ti and Al foils by self-propagating, high-temperature synthesis(SHS) in hot press. formation of TiAl 3 at the interface between Ti and Al foils was controlled by temperature, pressure, heating rate, and so on. According to the thermal analysis, it is known in this study that the heating rate is the most important factor to form the intermetallic compound by this SHS reaction. The V layer addition between Al and Ti foils increased SHS reaction temperatures. The fully dense, well-boned inter-metallic composite( TiA1/Ti 3 Al) sheets of 700 m thickness were formed by heat treatment at 1000 ? C for 10 hours after the SHS reaction of alternatively layered 10 Ti and 9 Al foils with the V coating layer. The phases and microstructures of intermetallic composite sheets were confirmed by EPMA and XRD.
Keywords:Ti-aluminide intermetallic compound;SHS reaction;TiA1/Ti 3 Al composite sheets;diffusion annealing;V addition
- Merzhanov AG, 'Self-Propagating High-Temperature Synthesis', Fizik. Khim. Sovrem. Problem, 6 (1983) (1983)
- Yamada O, Miyamoto Y, Koizumi M, Am. Ceram. Soc. Bull., 64(2), 319 (1985)
- Holt JB, Munir ZA, J. Mater. Sci., 21, 251 (1986)
- Kajuch J, Rigney JD, Lewandowski JJ, Mater. Sci. Eng., 155A, 59 (1992)
- Maupin HE, Rawers JC, J. Mater. Sci. Lett., 12, 540 (1993)
- Rawers JC, Hansen JS, Alman DE, Hawk JA, J. Mater. Sci. Lett., 13(18), 1357 (1994)
- Rawers RC, Alman DE, Hawk JA, Int. J. Self-Prop. High Temp. Syn., 2(1), 12 (1993)
- Banerjee D, Gogia AK, Nandy TK, Joshi VA, Acta Metall., 36, 871 (1988)
- Kattner VR, Botinger WJ, Mater. Sci. Eng., 152A, 9 (1992)
- Kim YW, J. Mat., 41, 24 (1989)
- Kim Y, Kim B, Nam T, Hur B, Kim Y, Korean J. Mater. Res., 8(11), 987 (1998)
- Maupin HE, Brawers JC, J. Mater. Sci. Lett., 12, 540 (1993)
- Brawers JC, Hansen JB, Alman DE, Hawk JA, Alman DE, J. Mater. Sci. Lett., 13, 1357 (1994)
- Sujata M, Bhargava S, Sangal S, J. Mater. Sci. Lett., 16(14), 1175 (1997)
- Alman DE, Brawers JC, Hawk JA, Metall. Mater. Trans. A, 26A, 589 (1995)
- Founelle JH, Donovan JJ, Kim S, Perepezko JH, Proceedings of 2nd Conference of the International Union of Microbeam Analysis Societies, Kailua-Kana, Hawaii, 425 (2000) (2000)
- Massalski TB, Binart Alloy Phase Diagram, Marray JL, Bennett SH, Baker H Eds., ASM, Materials Park, 1, 175 (1986) (1986)