From inorganic/organic nanocomposite based on chemically hybridized CdS-TGA to pure CdS nanoparticles

Fatemeh Davar; Mohammad Reza Loghman-Estarki; Rouholah Ashiri

Journal of Industrial and Engineering Chemistry, Vol.21, 965-970, January, 2015

DOI10.1016/j.jiec.2014.05.002 Export Citation

From inorganic/organic nanocomposite based on chemically hybridized CdS-TGA to pure CdS nanoparticles

Fatemeh Davar, Mohammad Reza Loghman-Estarki¹, and Rouholah Ashiri^{2, †}

Department of Chemistry, Isfahan University of Technology, Isfahan, Iran
¹Department of Material Engineering, Malek Ashtar University of Technology, Shahinshahr, Iran
²Department of Materials Science and Engineering, Dezful Branch, Islamic Azad University, P.O. Box 313, Dezful, Iran

E-mail:

The aim of this work is to synthesis and characterization of cadmium sulfide/ thioglycolic acid nanocomposite and its conversion to pure CdS nanoparticles. The products were characterized by X-ray diffraction (XRD), SEM, TEM, X-ray photoelectron spectroscopy (XPS) and Fourier transform infrared (FTIR) spectra. The CdS/organic nanocomposite was decomposed into pure wurtzite CdS nanoparticles through hydrothermal treatment at 200 ℃. UV-vis spectra were used to study the optical properties of CdS/organic nanocomposites and pure CdS. It was found that the absorption maximum of the CdS/TGA nanocomposite was significantly blue-shifted as compared to pure CdS nanoparticles.

Keywords:Cadmium sulfide;Nanocomposites;Nanowire;Hydrothermal

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[2] Zhang FY, Zhou Y, Cao Y, Chen J, Mater. Lett., 61, 4811 (2007)

[3] Liu Y, Xi G, Chen S, Zhang X, Zhu Y, Qian YT, Nanotechnology, 18, 285605 (2007)

[4] Zhang FY, Zhou YM, Sun YQ, Chen J, Ye XY, Huang JY, Mater. Res. Bull., 45(7), 859 (2010)

[5] Chen L, Zhu J, Li Q, Chen S, Wang Y, Eur. Polym. J., 43, 4593 (2007)

[6] Li D, Wang J, Li X, Liu H, Mater. Sci. Semicond. Process., 15, 152 (2012)

[7] Seoudi R, Kamal M, Shabaka AA, Abdelrazek EM, Eisa W, Synth. Met., 160, 479 (2010)

[8] Kim JY, Mulmi S, Lee CH, Park HB, Chung YS, Lee YM, J. Membr. Sci., 283(1-2), 172 (2006)

[9] Zhou X, Shi H, Fu X, Liu H, Zhao X, Hu Z, J. Dispersion Sci. Technol., 29, 250 (2008)

[10] Raut BT, Chougule MA, Nalage SR, Dalavi DS, Mali S, Patil PS, Patil VB, Ceram. Int., 38, 5501 (2012)

[11] Wang HM, Fang PF, Chen Z, Wang SJ, Appl. Surf. Sci., 253(20), 8495 (2007)

[12] Atay F, Bilgin V, Akyuz I, Kose S, Mater. Sci. Semicond. Process, 6, 197 (2003)

[13] Zhou MM, Yan SC, Shi Y, Yang M, Sun HB, Wang JY, Yin Y, Gao F, Appl. Surf. Sci., 273, 89 (2013)

[14] Yang J, Zeng JH, Yu SH, Yang L, Zhou GE, Qian YT, Chem. Mater., 12, 3259 (2000)

[15] Cao YL, Hu PF, Jia DZ, Appl. Surf. Sci., 265, 771 (2013)

[16] Bao C, Jin M, Lu R, Xue P, Zhang Q, Wang D, Zhao Y, J. Solid State Chem., 175, 322 (2003)

[17] Qin AM, Fang YP, Zhao WX, Liu HQ, Su CY, J. Cryst. Growth, 283(1-2), 230 (2005)

[18] Gao N, Guo F, Mater. Lett., 60, 3697 (2006)

[19] Lu W, Chen M, Wu LM, J. Colloid Interface Sci., 324(1-2), 220 (2008)

[20] Ge X, Ni Y, Zhang Z, Radiat. Phys. Chem., 64, 223 (2002)

[21] Salavati-Niasari M, Loghman-Estarki MR, Davar F, Inorg. Chim. Acta., 362, 3677 (2009)

[22] Chen F, Qiu WM, Chen XQ, Yang LG, Jiang XX, Wang M, Chen HZ, Sol. Energy, 85(9), 2122 (2011)

[23] Mondal SP, Dhar A, Ray SK, Mater. Sci. Semicond. Process, 10, 185 (2007)

[24] Yang W, Wu Z, Lu Z, Yang X, Song L, Microelectron. Eng., 83, 1971 (2006)

[25] Chen M, Pan L, Cao J, Ji H, Ji G, Ma X, Zheng Y, Mater. Lett., 60, 3842 (2006)

[26] Liu X, Liang X, Zhang N, Qiu G, Yi R, Mater. Sci. Eng. B-Solid State Mater. Adv. Technol., 132, 272 (2006)

[27] Zhang H, Yang DR, Ma XY, Ji YJ, Li SZ, Que DL, Mater. Chem. Phys., 93(1), 65 (2005)

[28] Salavati-Niasari M, Davar F, Loghman-Estarki MR, J. Alloy. Compd., 481, 776 (2009)

[29] Salavati-Niasari M, Loghman-Estarki MR, Davar F, Chem. Eng. J., 145(2), 346 (2008)

[30] Zhang H, Yang D, Sun H, Ma X, Que D, Mater. Lett., 60, 2004 (2006)

[31] Hedden RC, Bauer BJ, Smith AP, Grohn F, Amis E, Polymer, 43(20), 5473 (2002)

[32] Davar F, Mohammadikish M, Loghman MR, Cryst. Eng. Commun., 14, 7338 (2012)

[33] Mohammadikish M, Davar F, Loghman MR, Hamidi Z, Ceram. Int., 39, 3173 (2013)

[34] Zeng JY, Introduction to Quantum Mechanics, Peking University Press, Beijing, 1991.

[35] Wolf EL, Nanophysics and Nanotechnology: An Introduction to Modern Concepts in Nanoscience, Wiley-VCH, Weinheim, Germany, 2004.