화학공학소재연구정보센터
홈 로그인 로그아웃 연락처 사이트맵
Journal of Industrial and Engineering Chemistry, Vol.20, No.6, 3989-3993, November, 2014
DOI10.1016/j.jiec.2013.12.101  Export Citation
Flame atomic absorption spectrometric determination of Cd, Pb, and Cu in food samples after pre-concentration using 4-(2-thiazolylazo) resorcinol-modified activated carbon
Mohamed Habila, Erkan Yilmaz1, Zeid A. ALOthman, and Mustafa Soylak1, †
  • Chemistry Department, College of Science, King Saud University, Riyadh 11451, Saudi Arabia
  • 1Department of Chemistry, Science Faculty, Erciyes University, Kayseri 38039, Turkey
E-mail:
This work aimed to develop a solid-phase extraction method using low-cost activated carbon produced from waste and modified with 4-(2-thiazolylazo) resorcinol for Cd(II), Pb(II), and Cu(II). The results showed that quantitative recovery of analytes was obtained at pH 6 with 3 Mnitric acid as the eluent and a sample volume up to 1000 mL. The method was validated using certified reference material and addition-recovery tests. The limits of detection (LODs) for Pb(II), Cd(II), and Cu(II) were 2.03 μg L-1, 0.15 μg L-1, and 0.19 μg L-1, respectively. The procedure was applied for determination of analytes in food samples.
Keywords:Solid-phase extraction;Activated carbon;Heavy metals;Flame atomic absorption spectrometry
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