화학공학소재연구정보센터
Materials Science Forum, Vol.524-525, 223-228, 2006
The new and upgraded neutron instruments for material science at HMI -current activities in cooperation with industry
Recent progress in engineering includes the development of new materials and innovations in their processing and treatments. Material technologies, like the study of metals, alloys, ceramics and composites, especially non-destructive analyses of residual stresses profiles and textures, have gained an increasing importance. The dedicated residual stress diffractometers E3 and E7 at BENSC, HMI, Berlin are already equipped with new two-dimensional position sensitive detectors. An upgrade of the monochromator system is planned for 2006 which includes perfectly bent silicon crystals in order to optimise both intensity and angular resolution yielding a large gain of the diffractometer efficiency for strain measurements. A range of equipment for sample positioning is available, such as a closed Eulerian cradle for samples with weights of up to 5kg, a second cradle for heavy samples (up to 50 kg) with the ability to tilt the samples up to 90 degrees and a translation table carrying samples of up to 300kg and 1000mm in diameter. Gauge volumes can be adjusted by a new computer controlled variable slit-system in a range from 1x1x1 mm(3) up to several mm(3). In-situ residual stress analysis can be performed within industrial components during mechanical or thermal loading (up to 2000 K). Rapid data visualization as well as evaluation is performed by the specially designed software. The powder diffraction pattern is calculated by summation over the scattering angle dependent Debye-Scherrer lines on the two-dimensional 400*400 mm(2) planar area detector. A large amount of beam time is exclusively used for industrial research. Among the components that were investigated are crankshafts, impellers, pistons, cylinder heads, turbine blades and welds. Both instruments are similarly designed, where E3 is set up for higher flux and therefore penetration depths and E7 is designed for higher angular resolution.