Metal dispersed TiO2 nanocomposites were prepared by milling process. The microwave absorbing characteristics of the prepared nanocomposites with epoxy were studied in the 8.2-12.4 GHz frequency range for the microwave absorption application. The measured relative complex permittivity of metal dispersed nanocomposite-epoxy indicates higher values in comparison to the pure TiO2-epoxy nanocomposite. The Reflection loss (RL) values were calculated for thickness from 0.1 to 2.2 mm with an interval of 0.1 mm and the maximum value of RL found for TiO2-epoxy nanocomposite was -4.96 dB at 10.21 GHz frequency for 2.0 mm thickness. Whereas, RL value is improved to a maximum value of -13.67 dB at 10.13 GHz with Al dispersion (1.8 mm thickness) and -7.24 dB at 10.38 GHz with Ni dispersion (1.3 mm thickness). This study suggests the effectiveness metal particles dispersion for the development of thin microwave absorbers as well as increasing the level of RL. (C) 2013 The Society of Powder Technology Japan. Published by Elsevier B.V. and The Society of Powder Technology Japan. All rights reserved.