Journal of Industrial and Engineering Chemistry, Vol.20, No.4, 2287-2291, July, 2014
Surface functionalization of phosphazenenanosphere derivatives by Schiff-base-assisted metal complexes through a Si-spacer
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Surface functionalization of organometallic derivatives of phosphazenenanosphere (PNS) by the metal-coordinated Schiff base through (3-chloropropyl)trimethoxysilane as a silicon linker and spacer was investigated. The PNS’s derivative of 4,4'-sulfonyldiphenol (BPS) was added to Si-H2 saldien under ultrasonic irradiation. Metal ion (Mn2+, Ni2+ or Zn2+) was loaded on the PNS-Si-H2 saldien as desired metal salt. The structure and morphology was characterized by means of FT-IR, TGA, SEM, EDX and X-ray diffraction. The average diameters of nanosphere compounds are in the range of 250-300 nm.
Keywords:Surface functionalization;Phosphazenenanosphere;Metal-coordinated Schiff base;Si-spacer;Morphology and thermal stability
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