화학공학소재연구정보센터
Materials Chemistry and Physics, Vol.141, No.1, 208-215, 2013
Densification behaviour analysis of ZrO2 nanopowders for dental applications compacted by magnetic pulsed compaction
Sintered bulks of commercial ZrO2 nanopowders were produced by combined application of magnetic pulsed compaction (MPC) and subsequent two-step sintering, and finally, their density, hardness, shrinkage and formability were analyzed. The formability tests were conducted by a CAD/CAM system. Nearly fully dense (similar to 98%) commercial ZrO2 bulks were successfully obtained. With increasing MPC pressure, there was a decrease in the grain size of zirconia block. The ratio of PVA did not have a remarkable effect on the grain size. The optimum compaction pressure during MPC was 1 GPa and mixing conditions included using 1.0 wt. % PVA. The optimum processing condition included MPC process, followed by two-step sintering (first at 1000 and then at 1450 degrees C). The bulk under these conditions was found to have good formability, similar to 97% density, reasonable hardness (1150 Hv) and similar to 19% shrinkage. (C) 2013 Elsevier B.V. All rights reserved.