The solubility of 1H-1,2,4-triazole in ethanol, 1-propanol, 2-propanol, 1,2-propanediol, ethyl formate, methyl acetate, ethyl acetate, and butyl acetate at (283 to 363) K was measured using a laser monitoring observation technique. Results of these measurements were correlated with a semi-empirical equation. For the eight group data studied, the semi-empirical equation provided an accurate mathematical representation of the experimental data.