| 학회 |
한국공업화학회 |
| 학술대회 |
2009년 봄 (04/15 ~ 04/17, 호텔인터불고(대구)) |
| 권호 |
13권 1호 |
| 발표분야 |
무기재료 |
| 제목 |
Preparation and characterization of nanocrystalline porous SiC nano fiber from PAN and silica by electrospinning and carbothermal reduction |
| 초록 |
The nanocrystalline porous silicon carbide was prepared from various ratios with SiO2 and polyacrylonitrile by electrospinning and heat treatment. The electrospun fibers were converted to nanocrystalline porous silicon carbide by carbothermal reduction. Si elements in SiO2 and C elements in electrospun fibers were sintered to SiC fibers with escape of other elements like O, N, and H during carbothermal reduction. The escape of oxygen onto electrospun fiber led porous SiC fiber. The samples were characterized by XRD, SEM, BET, and TGA. The samples showed high SiC crystallite, high specific surface area, porosity and good oxygen resistance as a whole. |
| 저자 |
김상진1, 윤석민1, 강필현2, 전준표2, 이영석1
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| 소속 |
1충남대, 2한국원자력(연) |
| 키워드 |
SiC; SiO2; polyacrylonitrile; electrospinning
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| E-Mail |
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